时效工艺对冷变形多相紧固件GH350合金组织与性能的影响

材料工程与机械制造

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时效工艺对冷变形多相紧固件GH350合金组织与性能的影响

李科敏, 韩光炜, 邓波

钢铁研究总院高温材料研究所, 北京 100081

收稿日期:2011-09-01 修回日期:2011-11-14 出版日期:2012-06-25 发布日期:2012-06-26
通讯作者: 韩光炜 E-mail:guangwei_han@hotmail.com
基金资助:
国家级军品配套项目

Influence of Aging Treatment on Microstructure and Properties of Cold-drawn Alloy GH350

LI Kemin, HAN Guangwei, DENG Bo

Department of High Temperature Materials Research, Central Iron and Steel Research Institute, Beijing 100081, China

Received:2011-09-01 Revised:2011-11-14 Online:2012-06-25 Published:2012-06-26
Supported by:
National Military Project

摘要/Abstract

摘要： 利用光学显微镜和扫描电镜(SEM)分析,研究了冷拔态GH350(AEREX350)合金中η-Ni₃Ti相的时效析出规律以及对合金高温拉伸性能的影响。研究发现,冷拔态GH350合金中η-Ni₃Ti相在780~1 060 ℃温度范围内析出,且呈两种形态。晶界片状η相在780~1 060 ℃温度范围内均可析出,但在850~1 060 ℃温度区间,除晶界η相外,在晶内沿(111)面呈魏氏体形态析出片状η相。冷变形GH350合金在980 ℃开始发生再结晶,1 010 ℃可完全再结晶。对二阶时效后冷变形GH350合金的高温拉伸实验表明,随着一阶时效温度的升高,合金的高温塑性增加,强度降低。

关键词: 高温合金, η相, 再结晶, 时效, 高温拉伸试验, AEREX350合金

Abstract: The influence of aging treatment on the precipitation behavior of η-Ni₃Ti phase and high temperature tensile properties for cold-drawn alloy GH350 (AEREX350) is investigated by means of optical microscopy,scanning electron microscopy(SEM)and 730 ℃ tensile tests. It is found that η phase appears at grain boundaries or grain interiors during 780-1 060 ℃ aging in cold-drawn alloy GH350. The precipitation temperature of grain boundary η phase ranges from 780 ℃ to 1 060 ℃,while a Widmanstttan morphology of η phase aligning along (111) crystallographic planes of the matrix is formed at 850 ℃ to 1 060 ℃. Experimental results also show that cold-drawn alloy GH350 begins to recrystallize at 980 ℃,and has a complete recrystallization at 1 010 ℃. 730 ℃ tensile tests of cold-drawn alloy GH350 after a two-stage aging show that high temperature ductility of the alloy is improved,while the strength decreases with increase of the first stage aging temperature.

Key words: superalloys, &eta, phase, recrystallization, aging, high temperature tensile test, AEREX350 alloy

中图分类号:

V252.2
TG113

李科敏, 韩光炜, 邓波. 时效工艺对冷变形多相紧固件GH350合金组织与性能的影响[J]. 航空学报, 2012, (6): 1156-1162.

LI Kemin, HAN Guangwei, DENG Bo. Influence of Aging Treatment on Microstructure and Properties of Cold-drawn Alloy GH350[J]. ACTA AERONAUTICAET ASTRONAUTICA SINICA, 2012, (6): 1156-1162.

参考文献

[1] Doherty R D, Singh R P. Alloys containing gamma prime phase and particles and process for forming: U.S. Patent No. 5169463. 1992.

[2] Singh R P. Structure of thermo-mechanically processed multiphase alloys. Philadelphia,PA:Drexel University, 1987.

[3] Doherty R D, Singh R P. Alloys containing gamma prime phase and process for forming: U.S. Patent No. 4908069, 1990.

[4] Doherty R D, Singh R P, Slaney J S. Nickel-cobalt based alloys: U.S. Patent No. 4931255, 1990.

[5] Asgari S. Age-hardening behavior and phase identification in solution-treated AEREX350 superalloy. Metallurgical and Materials Transactions A, 2006,37(7); 2051-2057.

[6] Smith G D. Cobalt-nickel base alloys containing chromium and molybdenum: U.S.Patent No.3356542.1976.

[7] Pugliese L A, Stroup J P. A new Co-Ni-Mo-Cr ultrahigh-strength corrosion-resistant alloy system: multiphase. Cobalt, 1969,43(6): 80-86.

[8] Singh R P, Doherty R D. Strengthening in multiphase (MP35N) alloy: Part I. ambient temperature deformation and recrystallization. Metallurgical and Materials Transactions A, 1992,23(1): 307-319.

[9] Shaji E M, Kalidindi S R, Doherty R D. Influence of cold-work and aging heat treatment on strength and ductility of MP35N. Materials Science & Engineering A, 1999, 272(2): 371-379.

[10] Erickson G L, Muskegon M I. Nickel-cobalt based alloys: U.S.Patent No.5476555. 1995.

[11] Lu S Q, Shang B Z, Luo Z J, et al. Investigation on the cold deformation strengthening mechanism in MP159 alloy. Metallurgical and Materials Transactions A, 2000, 31(1): 5-13.

[12] Han G W. Microstructure variation of cold deformed MP159 alloy during aging. Journal of Materials Science and Technology, 1996,12(2): 109-113.

[13] Asgari S. Structure and strain hardening of superalloy AEREX350. Journal of Materials Processing Technology, 2001, 118(1-3): 246-250.

[14] Farvizi M, Asgari S. Effects of cold work prior to aging on microstructure of AEREX350 superalloy. Materials Science & Engineering A, 2008,480(1-2): 434-438.

[15] Samiee M, Asgari S. A TEM investigation on precipitation behavior of AEREX350 superalloy. Superalloys 2008. 2008: 549-552.

[16] Tomasello C M, Pettit F S, Birks N, et al. Precipitation behavior in AEREX350. Superalloys 1996. 1996:145-151.

[17] Hosseinifar M, Asgari S. Stactic recrystallization behavior of AEREX350 superalloy. Materials Science and Engineering A, 2010, 527(27-28): 7313-7317.

[18] Wan W J, Han G W, Deng B. Influence of aging treatment on precipitation behavior of η phase in Ni-Co-Cr alloy. Journal of Iron and Steel Research, International, 2010, 17(1):64-69,78.

[19] SPS Technologies Aerospace Fasteners Group. Superalloys developed by SPS technologies for aerospace fasteners. Jenkintown: SPS Technologies Inc.,1998.

[20] Li X Y, Zhang J, Rong L J, et al. The precipitation mechanism of secondary η phase in a FeNi-based superalloy. Chinese Journal of Materials Research, 2006,20(2):113-119.(in Chinese) 李秀艳,张建,戎利建, 等. Fe-Ni基合金中次生η相的析出机理. 材料研究学报,2006,20(2):113-119.

[21] Li X Y, Rong L J, Li Y Y. Effect of grain boundary η phase on the mechnical properties of Fe-Ni-Cr Alloy. Acta Metallurgica Sinica, 2005,41(11):1155-1158. (in Chinese) 李秀艳, 戎利建, 李依依. 晶界η相对Fe-Ni-Cr奥氏体合金力学性能的影响.金属学报,2005,41(11):1155-1158.

[22] Ge Y L, Zhang Y C, Hou C P. The effect of η phase in an iron-nickel base superalloy. Acta Metallurgica Sinica, 1979,15(2):197-202. (in Chinese) 葛云龙, 张永昌, 侯翠萍. 一种Fe-Ni基高温合金的η相.金属学报,1979,15(2):197-202.

[23] Han G W. Investigation on the recrystallization behaviour of cold deformed MP159 alloy. Journal of Materials Science and Technology, 1996, 12(4): 277-280.

E-mail：hkxb@buaa.edu.cn

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时效工艺对冷变形多相紧固件GH350合金组织与性能的影响

Influence of Aging Treatment on Microstructure and Properties of Cold-drawn Alloy GH350

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