中国飞机强度研究所建所 60 周年专刊

高温条件下FGH4108合金的保载-疲劳裂纹扩展行为

  • 秦豪 ,
  • 刘强 ,
  • 江荣 ,
  • 宋迎东 ,
  • 张强 ,
  • 刘建涛 ,
  • 邓健 ,
  • 卢天健
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  • 1.南京航空航天大学 多功能轻量化材料与结构工信部重点实验室,南京 210016
    2.南京航空航天大学 航空发动机热环境与热结构工信部重点实验室,南京 210016
    3.钢铁研究总院 高温材料研究所,北京 100081

收稿日期: 2025-06-03

  修回日期: 2025-06-17

  录用日期: 2025-07-07

  网络出版日期: 2025-07-15

基金资助

国家自然科学基金(12272174);国家科技重大专项(2017-Ⅵ-0008-0078);江苏省双创团队(JSSCTD202206);江苏省自然科学基金(BK20220136);航空发动机及燃气轮机基础科学中心重点项目(P2022-B-Ⅲ-007-001)

Dwell-fatigue crack growth behavior of FGH4108 alloy at high temperature

  • Hao QIN ,
  • Qiang LIU ,
  • Rong JIANG ,
  • Yingdong SONG ,
  • Qiang ZHANG ,
  • Jiantao LIU ,
  • Jian DENG ,
  • Tianjian LU
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  • 1.MIIT Key Laboratory of Multifunctional Lightweight Materials and Structures,Nanjing University of Aeronautics and Astronautics,Nanjing 210016,China
    2.MIIT Key Laboratory of Aero-engine Thermal Environment and Structure,Nanjing University of Aeronautics and Astronautics,Nanjing 210016,China
    3.High Temperature Material Institute,Central Iron and Steel Research Institute,Beijing 100081,China

Received date: 2025-06-03

  Revised date: 2025-06-17

  Accepted date: 2025-07-07

  Online published: 2025-07-15

Supported by

National Natural Science Foundation of China(12272174);Innovation and Entrepreneurship Teams of Jiangsu Province(JSSCTD202206);Natural Science Foundation of Jiangsu Province(BK20220136);National Science and Technology Major Project (2017-Ⅵ-0008-0078);Key Project of the Basic Science Center for Aero Engines and Gas Turbines (P2022-B-Ⅲ-007-001)

摘要

针对第4代粉末高温合金FGH4108,开展不同温度、不同保载时间下的疲劳裂纹扩展实验和中断实验研究,并结合扫描电子显微镜(SEM)、电子背散射衍射(EBSD)、电子探针X射线显微分析(EPMA)等表征手段分析温度和保载时间对裂纹扩展行为的影响,揭示氧化损伤对裂纹扩展的影响机理,提出1种描述机械-氧化耦合作用的疲劳裂纹扩展速率模型。结果表明:随着温度和保载时间增加,裂纹扩展速率上升,疲劳寿命显著下降;断面特征分析发现,在650 ℃时疲劳裂纹主要呈现穿晶扩展、断面平整,在750 ℃以上时疲劳裂纹主要呈现沿晶扩展、并伴随着二次裂纹的形成;同时,裂纹扩展过程中还伴随有尖端形貌改变与氧化物生成等现象,揭示了氧化作用对裂纹扩展的影响。提出的模型可以较好地描述不同温度与保载时间下的疲劳裂纹扩展速率,同时解耦了机械损伤、氧化损伤对裂纹扩展的影响,并确定了氧化损伤参数的温度相关性。

本文引用格式

秦豪 , 刘强 , 江荣 , 宋迎东 , 张强 , 刘建涛 , 邓健 , 卢天健 . 高温条件下FGH4108合金的保载-疲劳裂纹扩展行为[J]. 航空学报, 2025 , 46(21) : 532364 -532364 . DOI: 10.7527/S1000-6893.2025.32364

Abstract

Fatigue crack growth experiments and interrupted tests are conducted on the fourth-generation powder metallurgy superalloy FGH4108 under varying temperatures and dwell time. The influence of temperature and dwell time on crack growth behavior is analyzed using characterization techniques such as Scanning Electron Microscopy (SEM), Electron Backscatter Diffraction (EBSD), and Electron Probe Microanalysis (EPMA). The mechanism by which oxidation damage affects crack growth is revealed. A fatigue crack growth rate model describing the mechanical-oxidation coupling effect is proposed. The results show that as temperature and dwell time increase, the crack growth rate rises and fatigue life decreases significantly. Fractographic analysis reveals that at 650 ℃, fatigue cracks primarily propagate transgranularly with relatively flat fracture surfaces, while at temperatures above 750 ℃, fatigue cracks mainly propagate intergranularly, accompanied by the formation of secondary cracks. Concurrently, phenomena such as alterations in crack tip morphology and oxide formation were observed during crack propagation, elucidating the impact of oxidation on crack growth. The proposed model can better describe the fatigue crack growth rate at different temperatures and dwell time. At the same time, the effects of mechanical damage and oxidative damage on crack growth are decoupled, and the temperature dependence of oxidative damage parameters is determined.

参考文献

[1] PINEAU A, ANTOLOVICH S D. High temperature fatigue of nickel-base superalloys-A review with special emphasis on deformation modes and oxidation[J]. Engineering Failure Analysis200916(8): 2668-2697.
[2] REED R C. The superalloys: fundamentals and applications[M]. Cambridge: Cambridge University Press, 2008.
[3] 韩增祥. 温度对变形高温合金热疲劳性能的影响[J]. 燃气涡轮试验与研究200720(4): 53-57.
  HAN Z X. Effects of temperature on thermal fatigue properties of some wrought superalloys[J]. Gas Turbine Experiment and Research200720(4): 53-57 (in Chinese).
[4] ZHONG Z H, GU Y F, YUAN Y, et al. Fatigue crack growth behavior of a newly developed Ni-Co-base superalloy TMW-2 at elevated temperatures[J]. Materials Science and Engineering: A2012552: 464-471.
[5] LIU H, BAO R, ZHANG J Y, et al. A creep-fatigue crack growth model containing temperature and interactive effects[J]. International Journal of Fatigue201459: 34-42.
[6] WU C H, JIANG R, ZHANG L C, et al. Oxidation accelerated dwell fatigue crack growth mechanisms of a coarse grained PM Ni-based superalloy at elevated temperatures[J]. Corrosion Science2022209: 110702.
[7] TELESMAN J, GABB T P, GHOSN L J, et al. Effect of notches on creep-fatigue behavior of a P/M nickel-based superalloy[J]. International Journal of Fatigue201687: 311-325.
[8] CHEN X, PETTIT R G, DUDZINSKI D, et al. On the role of crack tip creep deformation in hot compressive dwell fatigue crack growth acceleration in aluminum and nickel engine alloys[J]. International Journal of Fatigue2021145: 106082.
[9] GABB T P, GAYDA J, TELESMAN J, et al. Factors influencing dwell fatigue life in notches of a powder metallurgy superalloy[J]. International Journal of Fatigue201348: 55-67.
[10] KIM D, JIANG R, REED P A S. Microstructural and oxidation effects on fatigue crack initiation mechanisms in a turbine disc alloy[J]. Journal of Materials Science202358(4): 1869-1885.
[11] BIKA D, MCMAHON C J. A model for dynamic embrittlement[J]. Acta Metallurgica et Materialia199543(5): 1909-1916.
[12] MOLINS R, HOCHSTETTER G, CHASSAIGNE J C, et al. Oxidation effects on the fatigue crack growth behaviour of alloy 718 at high temperature[J]. Acta Materialia199745(2): 663-674.
[13] VISKARI L, H?RNQVIST M, MOORE K L, et al. Intergranular crack tip oxidation in a Ni-base superalloy[J]. Acta Materialia201361(10): 3630-3639.
[14] ZHANG X B, LIU C S, LU J Y, et al. Secondarily precipitated phases of a Ni-based superalloy during durable thermal treatment[J]. Journal of Northeastern University200526(4): 355-358.
[15] 侯杰, 董建新, 姚志浩. GH4169合金高温疲劳裂纹扩展的微观损伤机制[J]. 工程科学学报201840(7): 822-832.
  HOU J, DONG J X, YAO Z H. Microscopic damage mechanisms during fatigue crack propagation at high temperature in GH4169 superalloy[J]. Chinese Journal of Engineering201840(7): 822-832 (in Chinese).
[16] MILLER C F, SIMMONS G W, WEI R P. Evidence for internal oxidation during oxygen enhanced crack growth in P/M Ni-based superalloys[J]. Scripta Materialia200348(1): 103-108.
[17] KITAGUCHI H S, LI H Y, EVANS H E, et al. Oxidation ahead of a crack tip in an advanced Ni-based superalloy[J]. Acta Materialia201361(6): 1968-1981.
[18] JIANG R, PROPRENTNER D, CALLISTI M, et al. Role of oxygen in enhanced fatigue cracking in a PM Ni-based superalloy: Stress assisted grain boundary oxidation or dynamic embrittlment [J]. Corrosion Science2018139: 141-154.
[19] 万煜玮, 周斌, 胡绪腾, 等. 某镍基粉末合金高温疲劳裂纹扩展行为与模型研究[J]. 推进技术202344(2): 262-271.
  WAN Y W, ZHOU B, HU X T, et al. High temperature fatigue crack growth behavior and model of a nickel-based powder metallurgy superalloy[J]. Journal of Propulsion Technology202344(2): 262-271 (in Chinese).
[20] EVANS J L, SAXENA A. Elevated temperature fatigue crack growth rate model for NI-BASE superalloys[J]. International Journal of Fracture2014185(1): 209-216.
[21] CHRIST H J, WACKERMANN K, KRUPP U. Effect of dynamic embrittlement on high temperature fatigue crack propagation in IN718-experimental characterisation and mechanism-based modelling[J]. Materials at High Temperatures201633(4/5): 528-535.
[22] WANG R Z, ZHU S P, WANG J, et al. High temperature fatigue and creep-fatigue behaviors in a Ni-based superalloy: Damage mechanisms and life assessment[J]. International Journal of Fatigue2018118: 8-21.
[23] HEIL M L. Crack growth in alloy 718 under thermal-mechanical cycling (fatigue, fracture, nickel, superalloy)[D]. Ohio: Air Force Institute of Technology, 1986.
[24] 徐超, 佴启亮, 姚志浩, 等. 晶界氧化对GH4738高温合金疲劳裂纹扩展的作用[J]. 金属学报201753(11): 1453-1460.
  XU C, NAI Q L, YAO Z H, et al. Grain boundary oxidation effect of GH4738 superalloy on fatigue crack growth[J]. Acta Metallurgica Sinica201753(11): 1453-1460 (in Chinese).
[25] VISKARI L, CAO Y, NORELL M, et al. Grain boundary microstructure and fatigue crack growth in Allvac 718Plus superalloy[J]. Materials Science and Engineering: A2011528(6): 2570-2580.
[26] CHAN K S, ENRIGHT M P, MOODY J, et al. A microstructure-based time-dependent crack growth model for life and reliability prediction of turbopropulsion systems[J]. Metallurgical and Materials Transactions A201445(1): 287-301.
[27] MA L Z, CHANG K M. Identification of SAGBO-induced damage zone ahead of crack tip to characterize sustained loading crack growth in alloy 783[J]. Scripta Materialia200348(9): 1271-1276.
[28] ENCINAS-OROPESA A, DREW G L, HARDY M C, et al. Effects of oxidation and hot corrosion in a nickel disc alloy[C]∥Superalloys 2008 Eleventh International Symposium. US: TMS, 2008: 609-618.
[29] CAO L Y, CHEN Y, SUN Y L, et al. Regional high temperature fatigue crack growth behavior of a microstructure-gradient nickel-based superalloy[J]. Materials Science and Engineering: A2024890: 145871.
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