航空学报 > 1993, Vol. 14 Issue (10): 490-495

氮化硅陶瓷的增韧研究

孙宏荣, 王明志   

  1. 北京航空航天大学第九研究室,北京 100083
  • 收稿日期:1992-04-14 修回日期:1992-11-05 出版日期:1993-10-25 发布日期:1993-10-25

STUDY ON TOUGHENING OF Si_3N_4 CERAMICS

Sun Hong-rong, Wang Ming-zhi   

  1. The Ninth Research Department, Beijing University of Aeronautics and Astrnautics, Beijing, 100083
  • Received:1992-04-14 Revised:1992-11-05 Online:1993-10-25 Published:1993-10-25

摘要: 研究了加入ZrO_2和SiC晶须对热压烧结Si_3N_4的增强增韧作用。加入ZrO_2和SiC晶须能提高复合材料的断裂韧性K_(IC),但降低了抗弯强度。分别加入10vol%纯ZrO_2和含有钇的Y-ZrO_2,使Si_3N_4陶瓷的室温K_(IC)从原来的6.3MPa·m~(1/2)分别提高到7.3MPa·m~(1/2)和7.6MPa·m~(1/2)。加入10wt%SiC晶须,使Si_3N_4陶瓷的室温K_(IC)从6.3MPa·m~(1/2)提高到7.1MPa·m~(1/2)。

关键词: 碳化硅晶须, 氧化锆, 增韧

Abstract: In this paper the influences of ZrO, and SiC Whiskers on strengthening and toughening effects of HP Si3N4 have been studied. By addition of ZrO2 and SiC whiskers, fracture toughness K IC, of composites increased, but flexural strength decreased simultaneously. In separate addition of 10vol% pure ZrO, and Y ZrO2 containing Y, fracture toughness of the Si3N4 ceramics at room temperature increased from 6.3 to 7.3 and 6.3 to 7.6 MPa m respectively. The improvement of fracture tonghness is due to the toughening effect of microcrack. By the way of addition of 10wt% SiC whiskers, at room temperature KIC of Si3N4 ceramics is increased from 6.3 to 7.1 MPa m . Toughening of SiC whisker was caused by crack deviation and pull-out effect of whiskers as well.

Key words: SiC whisker, zircoma toughening