Material Engineering and Mechanical Manufacturing

Measurement of Extinction Angle of Pyrocarbon by One Diagonal Quarter Intensity Principle

  • LI Yixian ,
  • QI Lehua ,
  • SONG Yongshan ,
  • LI Hejun ,
  • ZHANG Weihong
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  • 1. School of Mechanical Engineering, Northwestern Polytechnical University, Xi’an 710072, China;
    2. School of Materials Science and Engineering, Northwestern Polytechnical University, Xi’an 710072, China

Received date: 2011-08-24

  Revised date: 2011-09-20

  Online published: 2012-05-24

Supported by

National Natural Science Foundation of China (50832004,50972121, 50972120)

Abstract

In accordance with the extinction characteristics of pyrocarbons deposited around carbon fibers, this paper proposes a method for measurement of the extinction angle based on the one diagonal quarter intensity principle. It develops a dynamic template matching algorithm during image processing for the purpose of amending the bias of the observed patterns. Meanwhile, the problem of gray information extraction is solved for ellipse sections through rectifying the shape of fiber sections in image sequences. The proposed method can achieve the measurement of extinction angles accurately and effectively, which is suitable for both the condition of vertical section and inclined section. The errors between the values measured by the proposed method and observation are within 1?-2?, which increase with the degree of complexity of the polarized light microscopy (PLM) image texture.

Cite this article

LI Yixian , QI Lehua , SONG Yongshan , LI Hejun , ZHANG Weihong . Measurement of Extinction Angle of Pyrocarbon by One Diagonal Quarter Intensity Principle[J]. ACTA AERONAUTICAET ASTRONAUTICA SINICA, 2012 , (5) : 949 -955 . DOI: CNKI:11-1929/V.20111202.1032.004

References

[1] Oberlin A. Pyrocarbons. Carbon, 2002, 40(1): 7-24.
[2] Li H J. Carbon/carbon composites. New Carbon Materials, 2001, 16(2): 79-80. (in Chinese) 李贺军. C/C复合材料. 新型炭材料, 2001, 16(2): 79-80.
[3] Zhang J C, Luo R Y, Xiang Q, et al. Compressive fracture behavior of 3D needle-punched carbon/carbon composites. Materials Science and Engineering A, 2011, 528(15): 5002-5006.
[4] Hu Y J, Luo R Y, Zhang Y F, et al. Effect of preform density on densification rate and mechanical properties of carbon/carbon composites. Materials Science and Engineering A, 2010, 527(3): 797-801
[5] Reznik B, Guellali M, Gerthsen D, et al. Microstructure and mechanical properties of carbon-carbon composites with multilayered pyrocarbon matrix. Materials Letters, 2002, 52(1-2): 14-19.
[6] Xu H J, Huang B Y, Yi M Z, et al. Influence of matrix carbon texture on the temperature field of carbon/carbon composites during braking. Tribology International, 2011, 44(1): 18-24.
[7] Sun W C, Li H J, Zhang X L. Influence of high temperature treatment on microstructure and mechanical properties of 2D-C/C composites prepared by liquid-vaporized processing. Acta Aeronautica et Astronautica Sinica, 2002, 23(3): 276-278. (in Chinese) 孙万昌, 李贺军, 张秀莲. 高温处理对液相气化沉积碳/碳复合材料微观组织结构及力学性能的影响. 航空学报, 2002, 23(3): 276-278.
[8] Pfrang A, Wan Y Z, Schimmel T. Early stages of the chemical vapor deposition of pyrolytic carbon investigated by atomic force microscopy. Carbon, 2010, 48(3): 921-923.
[9] Wu X W, Luo R Y, Zhang J C, et al. Deposition mechanism and microstructure of pyrocarbon prepared by chemical vapor infiltration with kerosene as precursor. Carbon, 2009, 47(6): 1429-1435.
[10] Ge Y C, Yi M Z. Influence of carbon matrix on the tribology of C/C composites used as shaft sealing ring. Acta Aeronautica et Astronautica Sinica, 2004, 25(6): 619-624. (in Chinese) 葛毅成, 易茂中. 基体碳结构对轴间密封环用C/C复合材料摩擦磨损特性的影响. 航空学报, 2004, 25(6): 619-624.
[11] Xie W X, Qin A. The gray level resolution and intrinsic noise of human vision. Space Medicine & Medical Engineering, 1991, 4(1): 51-55. (in Chinese) 谢维信, 秦桉. 人的视觉对灰度级别的分辨能力及视觉内部噪声的研究. 航空医学与医学工程, 1991, 4(1): 51-55.
[12] Zhang W G, Hu Z J, Huttinger K J. Chemical vapor infiltration of carbon fiber felt: optimization of densification and carbon microstructure. Carbon, 2002, 40(14): 2529-2545.
[13] Li M L, Qi L H, Li H J, et al. Extinction angle for characterizing optical properties of pyrocarbon. Acta Aeronautica et Astronautica Sinica, 2008, 29(6): 1699-1704. (in Chinese) 李妙玲, 齐乐华, 李贺军, 等. 热解碳光学特性的消光角表征. 航空学报, 2008, 29(6): 1699-1704.
[14] Bortchagovsky E G. Reflection polarized light microscopy and its application to pyrolytic carbon deposits. Journal of Applied Physics, 2004, 95(9): 5192-5199.
[15] Bortchagovsky E G, Reznikb B, Gerthsenb D, et al. Optical properties of pyrolytic carbon deposits deduced from measurements of the extinction angle by polarized light microscopy. Carbon, 2003, 41(12): 2430-2433.
[16] Pfrang A, Schimmel T. Quantitative analysis of pyrolytic carbon films by polarized light microscopy. Surface and Interface Analysis, 2004, 36(2): 184-188.
[17] Li M L, Qi L H, Li H J, et al. Measurement of the extinction angle about laminar pyrocarbons by image analysis in reflection polarized light. Materials Science and Engineering A, 2007, 448(1-2): 80-87.
[18] Reznik B, Gerthsen D, Bortchagovsky E. An improved method for angular-resolved characterization of the optical anisotropy of pyrolytic carbon. Journal of Microscopy, 2006, 224(3): 322-327.
[19] Chuan X Y, Li H J, Lu J H. Why does cross-extinction property of pyrolytic carbon of C/C composites manufactured by CVI never disappear. Journal of Northwestern Polytechnical University, 2005, 23(5): 657-661. (in Chinese) 传秀云, 李贺军, 卢锦花. 化学气相渗透碳/碳复合材料热解碳光性特征——热解碳十字消光机理探讨. 西北工业大学学报, 2005, 23(5): 657-661.
[20] Liao J Q, Huang B Y, Huang Z F, et al. Microstructural characterization of pyrocarbon—polarized light microscopic observation of anisotropy of pyrocarbon. Physical Testing and Chemical Analysis: Physical Testing, 2002, 38(11): 501-506. (in Chinese) 廖寄乔,黄伯云,黄志锋,等. 热解碳微观结构的表征——热解碳各向异性的偏光分析. 理化检验:物理分册, 2002, 38(11): 501-506.
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