稀薄气体环境高灵敏度高稳定性压力敏感涂料开发与表征

  • 吴靖 ,
  • 陈培辉 ,
  • 黄赞强 ,
  • 黄峰 ,
  • 李国帅
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  • 1. 福州大学机械工程及自动化学院
    2. 中国空气动力研究与发展中心 高速空气动力研究所

收稿日期: 2024-10-25

  修回日期: 2024-12-17

  网络出版日期: 2024-12-18

Development and characterization of pressure-sensitive paint with high sensitivity and constancy in rarefied gas environments

  • WU Jing ,
  • CHEN Pei-Hui ,
  • HUANG Zan-Qiang ,
  • HUANG Feng ,
  • LI Guo-Shuai
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Received date: 2024-10-25

  Revised date: 2024-12-17

  Online published: 2024-12-18

摘要

在低压条件下准确测量航天器模型的表面压力分布,有助于对空间探测器进行优化设计。压力敏感涂料(PSP)是一种非接触式的全场表面压力分布光学测量技术。为了在稀薄气体环境中应用PSP技术,需要开发在低压条件下具有高压力灵敏度和高压力灵敏度稳定性的PSP以实现微小压力测量。本文以长发光寿命发光分子PdTFPP、高透氧聚合物室 温硫化硅橡胶(RTV)、结合不同种类和含量的微纳颗粒,开发压力敏感涂料,研究了颗粒种类、颗粒含量和分散剂对压力敏感涂料稳态性能的影响。实验结果表明采用介孔二氧化硅(mSiO2)作为微纳颗粒的聚合物-陶瓷压力敏感涂料 (PC-PSP),相较于其他微纳颗粒,表现出更高的压力灵敏度和更低的光降解率。颗粒含量达到70 wt%且不使用分散剂制备的PdTFPP/mSiO2-RTV,压力灵敏度和压力灵敏度稳定性分别为80.72 %/kPa和99.44%,并且其温度敏感度和光降解率分别为-0.9 %/K和-0.09 %/min。通过对比其它基于高氧透过性聚合物的PSP,证明了PdTFPP/mSiO2-RTV(70 wt%)更适用于低压条件下的稳态微小压力测量。

本文引用格式

吴靖 , 陈培辉 , 黄赞强 , 黄峰 , 李国帅 . 稀薄气体环境高灵敏度高稳定性压力敏感涂料开发与表征[J]. 航空学报, 0 : 1 -0 . DOI: 10.7527/S1000-6893.2024.31443

Abstract

Accurate measurement of the surface pressure distribution of spacecraft models under low-pressure conditions contrib-utes to the optimal design of space probes. Pressure-sensitive paint (PSP) is a non-contact optical measurement tech-nique for full-field surface pressure distribution. To apply PSP technology in rarefied gas environments, PSP with high pressure sensitivity and high pressure sensitivity constancy at low pressures needs to be developed. In this paper, the luminophore with long luminescence life, PdTFPP, the polymer with high oxygen permeability, room-temperature vulcan-ized silicone rubber (RTV), and micro-nano-particles with different types and contents are used to develop pressure-sensitive paints. The influences of particles type, particle contents, and dispersants on the static performances of the PSP are investigated. Experimental results indicate that the polymer-ceramic pressure-sensitive paint (PC-PSP) employing mesoporous silica (mSiO2) as the micro-nano-particles exhibits higher pressure sensitivity and lower photodegradation rate compared to other micro-nano-particles. PdTFPP/mSiO2-RTV with a particle content of 70 wt% and prepared with-out dispersant has a pressure sensitivity and pressure sensitivity constancy of 80.72 %/kPa and 99.44%, respectively, and its temperature sensitivity and photodegradation rate are -0.9 %/K and -0.09 %/min, respectively. In comparison to other PSP based on highly oxygen permeable polymers, PdTFPP/mSiO2-RTV (70 wt%) is demonstrated to be more suitable for static small pressure measurements in low pressure environments.

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